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HPLC-ECD System
HTEC-600
N E W
★ ★ ★
Ultra-High Sensitivity and Stability
超高感度 / 高安定
★ 感度はドーパミン・セロトニンで30fg 以下
★ 革新的セルの設計・無脈動ポンプのシステム設計
★ 冷却器とヒーターによる温度制御システム
★ ECDの最適化されたアプリケーション
all in One
一体型で省スペース
送液ポンプ、デガッサ、恒温槽、電気化学検出器 を一体化。
これにより流速が500μL/min を超える(カラムサイズが大きなもの)
ような他検出器の分析アプリケーションの実施が可能になりました
※ 従来のモデルでは庫内に入れる事が出来なかったサイズの長い
カラムも使用可能。幅広い分析アプリケーションに対応しました
作用電極の洗浄や交換・メンテナンスが容易
コンパクトでシンプルな設計の為、作用電極の交換をするのに工具は不要です。
またメンテナンスが驚くほど容易です。
purge
高速送液を行えます。稼働時間を設定できるので
液が枯れる心配はありません。エア抜き、液交換
を自動で行えるので一般的なHPLC のトラブル
で最も多いポンプによるエラーが大幅に改善
されました。
Timer
ポンプ、ECD それぞれを時間制御でON/OFF
する機能です。稼働時間を制限できるので移動
相の消費を最小限に抑える事が可能です。
このTIMER 機能によってポンプやECD を効率
的に稼働させスムーズなサンプル測定へ移行
する事が出来ます。
L.Switch
HTEC-600 からELS-500 を制御する事が可能
です。アミノ酸分析や比較的夾雑が出やすい
サンプルの場合クロマトグラム後半に出てくる
夾雑を除去することは分析の効率化につながる
ので、ELS-500を手軽に使用できることは実験
する上で大きなメリットとなります。
HTEC-600
HPLC-ECD SYSTEM
“仕様
<測定原理>***********************************************************************
方式 HPLC-ECD 法
<検出器>*************************************************************************
検出方式 アンペロメトリック
印加電圧 0 ~ ±2,000 mV、1 mV step
作用電極方式 薄層式
作用電極種類 グラファイト( 標準)、ピュアグラファイト、
グラシーカーボン、白金、金、銀
作用電極ガスケット TFE 製 厚さ25 μm または50 μm
参照電極 銀/ 塩化銀 (塩化リチウム封入液絡式)
対極 (補助電極) SUS316
接液部材質 PEEK、SUS316
記録計出力信号 ±10 V アナログ (0.1 nA = 1 mV)
時定数 1.0 sec、1.5 sec、3.0 sec
信号入力 SIGNAL IN: 接点信号300 msec 以上で検知
M.INJECTOR SIGNAL IN:オープン/ クローズ信号
切換えから300 sec で検知
外部機器制御信号 0 sec:信号入力検知と同時に接点信号 (1 sec) 出力
3 sec:信号入力検知から3 秒後に接点信号 (1 sec) 出力
6 sec:信号入力検知から6 秒後に接点信号 (1 sec) 出力
<送液ポンプ>*********************************************************************
送液方式 直列ダブルプランジャー往復動方式
1 ストローク容量 80 μL
ピストン材質 サファイア
設定流量範囲 1 ~ 3000 μL/min
安定流量範囲 100 ~ 2000 μL/min
接液部材質 PEEK、サファイア、ルビー、PTFE、PCTFE
耐圧 20 MPa
脈流低減機構 自動脈流制御
<脱気装置>***********************************************************************
方式 連続真空膜透過式
流路数 2 流路
内部容量 上段:約300 μL/ 流路
下段:約7.5 mL/ 流路
<恒温槽>*************************************************************************
方式 ペルチェ素子による加熱/ 冷却空気循環式
設定温度範囲 15 ~ 50℃ (1℃step)
温調精度 ±0.1℃
<全 体>***************************************************************************
寸法 290 W x 380 D x 435 H mm ( 突起部を含まず)
重量 23.2 kg
電源 AC 100 ~ 240 V 50/60 Hz 300 VA
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